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Second Edition

Making the Connections2: A How-To Guide

for Organic Chemistry Lab Techniques


Anne B. Padías, The University of Arizona

ISBN: 978-0-7380-4135-3
Net Price: $25.00

In this second edition of the popular text, Dr. Padías has enhanced existing content to address additional topic areas including 13C NMR, green chemistry, and molecular modeling.  She has also introduced end of the chapter/supplementary problems as well as a periodic table for reference.  A clear, concise writing style remains a hallmark of the second edition.
Through its precise presentation and practical approach, Making the Connections2 not only helps increase comprehension of the basic tenets but ignites a true
interest in organic techniques by offering many every-day examples of the chemical principles used in the lab.  MTC2 offers students an affordable alternative to comparative techniques guides.  It presents modern instrumentation techniques across various scales; universally suited as a supplement to any organic chemistry and lab curriculum.

Features

  • Priced well below comparable techniques manuals
  • Clear, concise descriptions of techniques on various scales
  • Includes basic principles, real life examples, and practical tips
  • Addition of 13C NMR, green chemistry, molecular modeling, and end of chapter/supplementary problems
  • Numerous instructional illustrations
  • 2-color,  6" x 9" soft-cover format

 

Table of Contents

Chapter 1 - First the Basics
  • ALWAYS Safety First
  • The Why and How of a Laboratory Notebook
  • Basic Lab Techniques
  • Solvents
  • Problems for Chapter 1
Chapter 2 - How to Identify Compounds
  • Phase Diagrams
  • Melting Point for Solids
  • Boiling Point for Volatile Liquids
  • Density of Liquids
  • Optical Rotation (Polarimetry)
  • Refractive Index
  • Elemental Analysis (Molecular Formula)
  • Spectroscopy Introduction
  • Infrared Spectroscopy
  • NMR
  • Ultraviolet Spectroscopy
  • Mass Spectrometry
  • Molecular Modeling
  • Problems for Chapter 2
Chapter 3 - Purification Techniques
  • Recrystallization
  • Extraction
  • Drying the Organic Fractions
  • Distillation
  • Sublimation
  • Chromatography
  • Thin Layer Chromatography
  • Column Chromatography
  • Other Column Chromatography Methods
  • Gas Chromatography
  • Problems for Chapter 3
Chapter 4 - Running a Reaction
  • Setup
  • Execution of the Reaction
  • The Workup
  • Primary Identification
  • Purification and Final Identification
  • Green Chemistry

Index

 

Additional Resources:

Also available, the companion Organic Chemistry Laboratory Manual by Dr. Padías.

Organic Chemistry Student Lab Notebook


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